Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Bromide | HCID 6323 | — |
| Reactant | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 131731240 | HCID 131731240 | — |
Reaction Steps
A bottle containing methyl bromide (MeBr; b.p. 4° C.) was cooled down to −10° C. MeBr (50.00 mL) was poured out and weighed (88.53 g; d=1.77 g/mL). The methyl bromide was added into a pre-cooled bottle containing 1-Methyl-2-Pyrrolidinone (NMP) {50.00 mL; 54.39 g, −10° C.} to form approximately 100 mL solution at −10° C. (MeBr/NMP).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09415044B2 |
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| Source dataset | uspto-grants-2016_08 |
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| ORD ID | ord-724ccae2660b4cde9578beed1de86e82 |
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| Source note | uspto-grants-2016_08 |
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