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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1482460Generated: November 1, 2026

Methyl Bromide → HCID 131731240, compound

https://huagongshe.com/reaction/1482460

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl BromideHCID 6323—
ReactantN-methyl-2-pyrrolidoneHCID 13387—
ProductHCID 131731240HCID 131731240—

Reaction Conditions

Temperature-10 °C

Reaction Steps

A bottle containing methyl bromide (MeBr; b.p. 4° C.) was cooled down to −10° C. MeBr (50.00 mL) was poured out and weighed (88.53 g; d=1.77 g/mL). The methyl bromide was added into a pre-cooled bottle containing 1-Methyl-2-Pyrrolidinone (NMP) {50.00 mL; 54.39 g, −10° C.} to form approximately 100 mL solution at −10° C. (MeBr/NMP).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09415044B2
Source datasetuspto-grants-2016_08
ORD IDord-724ccae2660b4cde9578beed1de86e82
Source noteuspto-grants-2016_08