Glutaric Acid → Lauryl acrylate

HRID 1482749Notes

Reaction equation

HRID 1482749 reaction equation
[C:1](O)(=O)CCCC(O)=O.C(O)COCCO.[C:17]([OH:19])#[CH:18].C[O:21][C:22]1C=[C:24](/[CH:29]=[CH:30]/[C:31](/O)=[CH:32]/[C:33](/[CH:35]=[CH:36]/C2C=CC(O)=C(OC)C=2)=O)[CH:25]=[CH:26][C:27]=1O>O>[C:17]([O:21][CH2:22][CH2:27][CH2:26][CH2:25][CH2:24][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:35][CH3:36])(=[O:19])[CH:18]=[CH2:1]

Participants

5

Reactant 3

HCID 743Glutaric AcidHCID 8117Diethylene GlycolHCID 137222797HCID 137222797, compound

Product 1

HCID 75084Lauryl acrylate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Glutaric acid (10 parts), diethylene glycol (10 parts), Acetylenol E100 (surfactant produced by Kawaken Fine Chemicals Co., Ltd.) (1 part), and ion exchange water (79 parts) were mixed and thoroughly stirred. Then the mixture was pressure-filtered through a microfilter (produced by FUJIFILM Holdings Corporation) with a 3.0 μm pore size. As a result, a liquid composition was obtained.

Workup

  1. filtrationThen the mixture was pressure-filtered through a microfilter (produced by FUJIFILM Holdings Corporation) with a 3.0 μm pore size
  2. customAs a result, a liquid composition was obtained

Sources & evidence

ORD record
ord-da5189fd32244fef823196b16246edb1
Source dataset
uspto-grants-2016_08
Patent number
US09415581B2

Reaction notes

Loading…