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HRID1482806

反应详情

EQUATION

反应方程式

HRID 1482806 的结构方程式

REACTANTS

反应物

2
结构：CNc1ccc(Cl)cc1
HCID70272

4-Chloro-N-methylaniline

C7H8ClN

结构：O=C(O)c1ccc(S(=O)(=O)Cl)cc1
HCID82385

Benzoic acid, 4-(chlorosulfonyl)-

C7H5ClO4S

PRODUCTS

生成物

1
结构：CN(c1ccc(Cl)cc1)S(=O)(=O)c1ccc(C(=O)O)cc1
HCID60008486

未命名化合物

PROCEDURE

实验过程

4-(chlorosulfonyl)benzoic acid (0.5 g, 2.27 mmol) was treated with 4-chloro-N-methylaniline (963 mg, 6.80 mmol) using method A to give 4-(N-(4-chlorophenyl)-N-methylsulfamoyl)benzoic acid as a white solid. Yield: 406 mg (55%). 1H-NMR: 8.11 (d, J=8.5 Hz, 2H), 7.63 (d, J=8.5 Hz, 2H), 7.42 (d, J=8.5 Hz, 2H), 7.14 (d, J=8.5 Hz, 2H), 3.15 (s, 3H).