HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 90135691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 90134892 | HCID 90134892 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90135691 | HCID 90135691 | 98.2% |
Reaction Steps
Dissolve 1-cyclopropyl-2-((2,2-dimethyl-1,3-dioxolan-4-yl)methoxy)ethanol (1.1 g, 5.09 mmol) in MeOH (20 mL) and add HCl (1 M in Et2O; 18 mL, 18 mmol). Stir at ambient temperature for 3 hours. Concentrate under reduced pressure to provide the title product (880 mg, 98.2%) as a colorless oil. MS (m/z): 199 (M+23).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09416138B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-e97ec8992b40460c82391e8c774443ad |
| Source note | uspto-grants-2016_08 |