Allyl bromide → HCID 22397836, compound

HRID 1483906Notes

Reaction equation

HRID 1483906 reaction equation
[CH3:1][S:2]([C:5]1[CH:6]=[C:7]([CH:11]2[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]2)[CH:8]=[CH:9][CH:10]=1)(=[O:4])=[O:3].[CH2:17](Br)[CH:18]=[CH2:19]>>[CH2:19]([N:14]1[CH2:15][CH2:16][CH:11]([C:7]2[CH:8]=[CH:9][CH:10]=[C:5]([S:2]([CH3:1])(=[O:4])=[O:3])[CH:6]=2)[CH2:12][CH2:13]1)[CH:18]=[CH2:17]

Participants

3

Reactant 2

HCID 7841Allyl bromideHCID 129889574-(3-(Methylsulfonyl)phenyl)piperidine

Product 1

HCID 22397836HCID 22397836, compound

Procedure

Beginning with 4-(3-methanesulfonyl-phenyl)-piperidine and allylbromide, the titled compound was recovered by the procedure described in Example 1. MS m/z (relative intensity, 70 eV) 279 (M+, 74), 96 (bp), 82 (98), 68 (74), 55 (93). Rf=0.42 (MeOH, 0.08 (EtOAc).

Workup

  1. customthe titled compound was recovered by the procedure

Sources & evidence

ORD record
ord-7f80a4dccd92432f9357103001d1391d
Source dataset
uspto-grants-2016_08
Patent number
USRE046117E1

Reaction notes

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