1-Bromo-4-nitrobenzene → HCID 53248133, compound

HRID 1484066Notes

Reaction equation

HRID 1484066 reaction equation
[CH2:1]([O:9][CH2:10][CH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].BrC1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1>>[CH:11]1([CH2:10][O:9][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]2[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=2)[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]1

Participants

3

Reactant 2

HCID 114661-Bromo-4-nitrobenzeneHCID 53248071HCID 53248071, compound

Product 1

HCID 53248133HCID 53248133, compoundYield 65%

Procedure

General procedure M was used to convert 5.73 mmol of 11 and 6.30 mmol of 1-bromo-4-nitrobenzene to 3.72 mmol (65%) of the title compound.

Sources & evidence

ORD record
ord-0483e5ed2d7f42b9bd478404d740e9a3
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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