1-Bromo-4-nitrobenzene → HCID 53248131, compound

HRID 1484068Notes

Reaction equation

HRID 1484068 reaction equation
[CH2:1]([O:8][CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH:6]=[CH2:7].Br[C:17]1[CH:22]=[CH:21][C:20]([N+:23]([O-:25])=[O:24])=[CH:19][CH:18]=1>>[CH2:9]([O:8][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:17]1[CH:22]=[CH:21][C:20]([N+:23]([O-:25])=[O:24])=[CH:19][CH:18]=1)[C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

3

Reactant 2

HCID 114661-Bromo-4-nitrobenzeneHCID 53248068HCID 53248068, compound

Product 1

HCID 53248131HCID 53248131, compoundYield 68.3%

Procedure

General procedure M was used to convert 5.90 mmol of 11a and 6.49 mmol of 1-bromo-4-nitrobenzene to 4.03 mmol (68%) of the title compound.

Sources & evidence

ORD record
ord-fc1c6634fd8d4ba091de0951ffb0d718
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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