1-Bromo-4-nitrobenzene → HCID 53248132, compound

HRID 1484070Notes

Reaction equation

HRID 1484070 reaction equation
[CH2:1]([O:7][CH2:8][CH:9]1[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1)[CH2:2][CH2:3][CH2:4][CH:5]=[CH2:6].Br[C:16]1[CH:21]=[CH:20][C:19]([N+:22]([O-:24])=[O:23])=[CH:18][CH:17]=1>>[CH:9]1([CH2:8][O:7][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:16]2[CH:21]=[CH:20][C:19]([N+:22]([O-:24])=[O:23])=[CH:18][CH:17]=2)[CH2:10][CH2:11][CH2:12][CH2:13][CH2:14]1

Participants

3

Reactant 2

HCID 114661-Bromo-4-nitrobenzeneHCID 68182751HCID 68182751, compound

Product 1

HCID 53248132HCID 53248132, compoundYield 26%

Procedure

General procedure M was used to convert 5.21 mmol of 11b and 5.73 mmol of 1-bromo-4-nitrobenzene to 1.35 mmol (26%) of the title compound.

Sources & evidence

ORD record
ord-0defe3b79c884e08af7b6ccef18da63e
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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