1-Cyanocyclopropanecarboxylic acid → HCID 53248232, compound

HRID 1484073Notes

Reaction equation

HRID 1484073 reaction equation
[CH:1]1([CH2:7][O:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]2[CH:23]=[CH:22][C:20]([NH2:21])=[CH:19][CH:18]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[C:24]([C:26]1([C:29](O)=[O:30])[CH2:28][CH2:27]1)#[N:25]>>[C:24]([C:26]1([C:29]([NH:21][C:20]2[CH:22]=[CH:23][C:17]([CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][O:8][CH2:7][CH:1]3[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]3)=[CH:18][CH:19]=2)=[O:30])[CH2:28][CH2:27]1)#[N:25]

Participants

3

Reactant 2

HCID 27332591-Cyanocyclopropanecarboxylic acidHCID 53248184HCID 53248184, compound

Product 1

HCID 53248232HCID 53248232, compoundYield 98%

Procedure

General procedure E was used to convert 2.05 mmol of 13c and 3.08 mmol of 1-cyanocyclopropanecarboxylic acid to 2.01 mmol (98%) of the title compound.

Sources & evidence

ORD record
ord-715b5cf5e6ae46beab4d375fc74b98e7
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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