1-Bromo-4-nitrobenzene → HCID 66927367, compound

HRID 1484074Notes

Reaction equation

HRID 1484074 reaction equation
[CH2:1]([O:8][CH2:9][CH:10]1[CH:17]2[CH2:18][CH:13]3[CH2:14][CH:15]([CH2:19][CH:11]1[CH2:12]3)[CH2:16]2)[CH2:2][CH2:3][CH2:4][CH2:5][CH:6]=[CH2:7].Br[C:21]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][CH:22]=1>>[N+:27]([C:24]1[CH:25]=[CH:26][C:21]([CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][O:8][CH2:9][CH:10]2[CH:17]3[CH2:18][CH:13]4[CH2:14][CH:15]([CH2:19][CH:11]2[CH2:12]4)[CH2:16]3)=[CH:22][CH:23]=1)([O-:29])=[O:28]

Participants

3

Reactant 2

HCID 114661-Bromo-4-nitrobenzeneHCID 66927433HCID 66927433, compound

Product 1

HCID 66927367HCID 66927367, compoundYield 47%

Procedure

General procedure M was used to convert 2.77 mmol of 11d and 3.05 mmol of 1-bromo-4-nitrobenzene to 1.30 mmol (47%) of the title compound.

Sources & evidence

ORD record
ord-95a90e96bf534208a155720192c8c187
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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