1-Bromo-4-nitrobenzene → HCID 14931617, compound

HRID 1484076Notes

Reaction equation

HRID 1484076 reaction equation
[CH2:1]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH:8]=[CH2:9].Br[C:17]1[CH:22]=[CH:21][C:20]([N+:23]([O-:25])=[O:24])=[CH:19][CH:18]=1>>[N+:23]([C:20]1[CH:21]=[CH:22][C:17]([CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)=[CH:18][CH:19]=1)([O-:25])=[O:24]

Participants

3

Reactant 2

HCID 114661-Bromo-4-nitrobenzeneHCID 18786517HCID 18786517, compound

Product 1

HCID 14931617HCID 14931617, compoundYield 54%

Procedure

General procedure M was used to convert 5.08 mmol of 15 and 5.59 mmol of 1-bromo-4-nitrobenzene to 2.74 mmol (54%) of the title compound.

Sources & evidence

ORD record
ord-cac2d9c026f04ca98ce4e5341378e879
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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