1-Bromo-4-nitrobenzene → HCID 53248319, compound

HRID 1484078Notes

Reaction equation

HRID 1484078 reaction equation
[CH2:1]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH:7]=[CH2:8].Br[C:16]1[CH:21]=[CH:20][C:19]([N+:22]([O-:24])=[O:23])=[CH:18][CH:17]=1>>[N+:22]([C:19]1[CH:20]=[CH:21][C:16]([CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][CH2:1][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:17][CH:18]=1)([O-:24])=[O:23]

Participants

3

Reactant 2

HCID 114661-Bromo-4-nitrobenzeneHCID 12003083HCID 12003083, compound

Product 1

HCID 53248319HCID 53248319, compoundYield 71%

Procedure

General procedure M was used to convert 5.31 mmol of 15a and 5.84 mmol of 1-bromo-4-nitrobenzene to 3.42 mmol (71%) of the title compound.

Sources & evidence

ORD record
ord-6bc266e63eaf403090eae689fa384856
Source dataset
uspto-grants-2016_08
Patent number
US09421177B2

Reaction notes

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