Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Fluoro-4-(perfluoroethyl)benzoic acid | HCID 46941350 | — |
| Product | HCID 90315066 | HCID 90315066 | 93.4% |
Reaction Steps
To 2-fluoro-4-(1,1,2,2,2-pentafluoroethyl)benzoic acid (1 g, 3.87 mmol) was added thionyl chloride (3.67 mL, 50.36 mmol) and the reaction was stirred at 60° C. for 22 hours. Excess thionyl chloride was removed in vacuo to yield 2-fluoro-4-(1,1,2,2,2-pentafluoroethyl)benzoyl chloride (1 g, 93%) as a viscous yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09421196B2 |
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| Source dataset | uspto-grants-2016_08 |
|---|
| ORD ID | ord-474a27e6b3d744aea3c360023f7d21a8 |
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| Source note | uspto-grants-2016_08 |
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