HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 3-Amino-1,2,4-triazine mesylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 3-(benzyloxy)benzoate | HCID 13368031 | — |
| Reactant | HCID 178505340 | HCID 178505340 | — |
| Product | 3-Amino-1,2,4-triazine mesylate | HCID 86649731 | — |
Reaction Steps
Prepared by reacting acenaphthenequinone (3) with aminoguanidine bismesylate for 24 hrs using the above procedure except that the basification step with ammonia was omitted. The title compound was obtained as bright yellow prisms in 83.2%, mpt=264-266° (froth)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422253B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-a8de5f0905094df09005f1c293579976 |
| Source note | uspto-grants-2016_08 |