HCID 90014581, compound → HCID 62475748, compound
Reaction equation
CC1C(OC2C=CC=C(CCC)C=2)=NC=C([N+]([O-])=O)C=1.[CH3:21][C:22]1[C:23]([O:31][C:32]2[CH:37]=[CH:36][CH:35]=[C:34]([O:38][CH2:39][CH3:40])[CH:33]=2)=[N:24][CH:25]=[C:26]([N+:28]([O-])=O)[CH:27]=1>>[NH2:28][C:26]1[CH:27]=[C:22]([CH3:21])[C:23]([O:31][C:32]2[CH:37]=[CH:36][CH:35]=[C:34]([O:38][CH2:39][CH3:40])[CH:33]=2)=[N:24][CH:25]=1Participants
3
Procedure
The title compound was prepared in a similar way with respect to Intermediate 26 replacing 3-methyl-5-nitro-2-{[3-(2-methylethyl)phenyl]oxy}-pyridine (Intermediate 24) with 3-methyl-5-nitro-2-{[3-(ethyloxy)phenyl]oxy}-pyridine (Intermediate 25).
Sources & evidence
- ORD record
- ord-a9f9f066b212438299b8d324177b1b58
- Source dataset
- uspto-grants-2016_08
- Patent number
- US09422252B2
Reaction notes
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