HuagongsheHuagongshe Chemistry Print Report · For research reference only
sodium (1Z)-1-cyanoprop-1-en-2-olate → HCID 178467934, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | sodium (1Z)-1-cyanoprop-1-en-2-olate | HCID 23687916 | — |
| Reactant | HCID 178434325 | HCID 178434325 | — |
| Product | HCID 178467934 | HCID 178467934 | — |
Reaction Steps
Following the procedure described for Example 2A, the title compound was prepared using 2.74 g (15.5 mmol) 6-fluoro-3-methyl-1H-indazole-5-carbaldehyde (Example 3A) and 2.6 g (24.8 mmol) sodium (1Z)-1-cyanoprop-1-en-2-olate to yield 1.6 g (42% of th.) of the crude product which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422263B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-4319f0b4d7a74d48a74aa35e65317233 |
| Source note | uspto-grants-2016_08 |