HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → HCID 118113213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | 2-Methyl-5-hydroxypyridine | HCID 14275 | — |
| Reactant | (Bromomethyl)cyclobutane | HCID 2734658 | — |
| Reactant | [4-(Chloromethyl)phenyl]methanol | HCID 5107660 | — |
| Product | HCID 118113213 | HCID 118113213 | 113.7% |
Reaction Steps
Instead of 4-hydroxybenzaldehyde and (bromomethyl)cyclobutane, 5-hydroxy-2-methylpyridine (767 mg) and 4-(chloromethyl)benzyl alcohol (1.00 g) were respectively used and treated by the same techniques as in Reference Examples 9-1 and 19-1 to give the titled compound as a pale yellow solid (1.65 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422240B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-66133493b56049efaed3a9c295c4da15 |
| Source note | uspto-grants-2016_08 |