HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)benzoic acid → HCID 11820034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)benzoic acid | HCID 22599 | — |
| Reactant | Methanamine, N-methoxy-, hydrochloride (1:1) | HCID 81138 | — |
| Reactant | Cyclopropaneacetic acid | HCID 138440 | — |
| Reactant | 4-Piperidinemethanol | HCID 420771 | — |
| Product | HCID 11820034 | HCID 11820034 | 73% |
Reaction Steps
Instead of 4-(bromomethyl)benzoic acid and N,O-dimethylhydroxylamine hydrochloride, cyclopropylacetic acid (869 mg) and 4-piperidinemethanol (1.00 g) were respectively used and treated by the same technique as in Reference Example 16-1(1) to give the titled compound as a colorless oil (1.25 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09422240B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-ee283096b1f04e8e9a922ab8fef78a90 |
| Source note | uspto-grants-2016_08 |