Diethyl dibromoterephthalate → Dimethyl 2,5-bis-(9'-phenyl-9'H-[3,3']bicarbazolyl-9-yl)terephthalate

Participants

Reaction Steps

The compound is synthesised by the same procedure as for the corresponding step of Example 5 by reaction of 13.6 g (43 mmol) of diethyl dibromoterephthalate and 39 g (95.9 mmol) of 9-phenyl-3,3′-bicarbazole. The pure product is obtained by recrystallisation. The yield is 31 g (31 mmol), corresponding to 80% of theory.

Provenance & Evidence