N-Methylethylamine → N'-(4-Bromophenyl)-N-ethyl-N-methyl-methanesulfonimidamide

HRID 1485613Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])=[O:10])=[CH:4][CH:3]=1.[CH3:12][NH:13][CH2:14][CH3:15]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]=[S:9]([CH3:11])([N:13]([CH2:14][CH3:15])[CH3:12])=[O:10])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 12219N-Methylethylamine

HCID 14195208N-(4-Bromophenyl)methanesulfinamide

Product 1

HCID 118863958N'-(4-Bromophenyl)-N-ethyl-N-methyl-methanesulfonimidamide

Procedure

The title compound is prepared from N-(4-bromophenyl)methanesulfinamide and methylethylamine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.99 min; Mass spectrum (ESI+): m/z=291, 293 [M+H]+.

Sources & evidence

ORD record: ord-a8edcd2086114f08841cc61df80eee51
Source dataset: uspto-grants-2016_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09422312B2

Reaction notes

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