Azetidine → N-[Azetidin-1-yl(methyl)oxo-lambda6-sulfanylidene]-4-bromoaniline

HRID 1485615Notes

Reaction equation

HRID 1485615 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])=[O:10])=[CH:4][CH:3]=1.[NH:12]1[CH2:15][CH2:14][CH2:13]1>>[N:12]1([S:9]([CH3:11])(=[O:10])=[N:8][C:5]2[CH:6]=[CH:7][C:2]([Br:1])=[CH:3][CH:4]=2)[CH2:15][CH2:14][CH2:13]1

Participants

3

Reactant 2

HCID 10422AzetidineHCID 14195208N-(4-Bromophenyl)methanesulfinamide

Product 1

HCID 118863933N-[Azetidin-1-yl(methyl)oxo-lambda6-sulfanylidene]-4-bromoaniline

Procedure

The title compound is prepared from N-(4-bromophenyl)methanesulfinamide and azetidine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.92 min; Mass spectrum (ESI+): m/z=289, 291 [M+H]+.

Sources & evidence

ORD record
ord-9e7e44c468b54107971b1c5ebc84ba9a
Source dataset
uspto-grants-2016_08
Patent number
US09422312B2

Reaction notes

Loading…