Ethylamine → HCID 118863949, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])=[O:10])=[CH:4][CH:3]=1.[CH2:12]([NH2:14])[CH3:13]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])(=[N:14][CH2:12][CH3:13])=[O:10])=[CH:4][CH:3]=1Participants
3
Procedure
The title compound is prepared from N-(4-bromophenyl)methanesulfinamide and ethylamine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.91 min; Mass spectrum (ESI+): m/z=277, 279 [M+H]+.
Sources & evidence
- ORD record
- ord-011b0eeed3834c51b3fe18f10c4a8bae
- Source dataset
- uspto-grants-2016_08
- Patent number
- US09422312B2
Reaction notes
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