5-Amino-2-chloropyridine → HCID 118863923, compound

HRID 1485625Notes

Reaction equation

HRID 1485625 reaction equation
[NH2:1][C:2]1[CH:3]=[CH:4][C:5]([Cl:8])=[N:6][CH:7]=1.[CH3:9][S:10](Cl)=[O:11]>>[Cl:8][C:5]1[N:6]=[CH:7][C:2]([NH:1][S:10]([CH3:9])=[O:11])=[CH:3][CH:4]=1

Participants

3

Reactant 2

HCID 793055-Amino-2-chloropyridineHCID 548463Methanesulfinyl chloride

Product 1

HCID 118863923HCID 118863923, compound

Procedure

The title compound is prepared from 5-amino-2-chloropyridine and methanesulfinyl chloride following a procedure analogous to that described for Intermediate 3 (Step 1). LC (method 1): tR=0.82 min; Mass spectrum (ESI+): m/z=191 [M+H]+.

Sources & evidence

ORD record
ord-ccd51e0581874ef4a24bad9e4dc6fee7
Source dataset
uspto-grants-2016_08
Patent number
US09422312B2

Reaction notes

Loading…