Dimethylamine → HCID 118863922, compound

HRID 1485626Notes

Reaction equation

HRID 1485626 reaction equation
[Cl:1][C:2]1[N:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])=[O:10])=[CH:4][CH:3]=1.[CH3:12][NH:13][CH3:14]>>[Cl:1][C:2]1[N:7]=[CH:6][C:5]([N:8]=[S:9]([CH3:11])([N:13]([CH3:14])[CH3:12])=[O:10])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 118863923HCID 118863923, compound

Product 1

HCID 118863922HCID 118863922, compound

Procedure

The title compound is prepared from N-(6-chloropyridin-3-yl)methanesulfinamide and dimethylamine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.78 min; Mass spectrum (ESI+): m/z=234 [M+H]+.

Sources & evidence

ORD record
ord-c15a8ad609694039ae42b560d52be407
Source dataset
uspto-grants-2016_08
Patent number
US09422312B2

Reaction notes

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