HCID 118863947, compound → HCID 131736744, compound

Participants

Reaction Steps

The title compound is prepared from (3R,3aR,6R,6aR)-6-(6-chloro-5-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-3-(2-trimethylsilanyl-ethoxymethyl)-3H-imidazo[4,5-b]pyridin-2-yloxy)hexahydrofuro[3,2-b]furan-3-ol and N′-(6-chloropyridin-3-yl)-N-methyl-methanesulfonimidamide following a procedure analogous to that described for Intermediate 13 (Step 3) using 1,2-dimethoxyethane as a solvent. LC (method 1): tR=0.96 min; Mass spectrum (ESI+): m/z=687 [M+H]+.

Provenance & Evidence