Dimethylamine → HCID 118863962, compound

HRID 1485633Notes

Reaction equation

HRID 1485633 reaction equation
[Cl:1][C:2]1[N:7]=[CH:6][C:5]([NH:8][S:9]([CH3:11])=[O:10])=[CH:4][N:3]=1.[CH3:12][NH:13][CH3:14]>>[Cl:1][C:2]1[N:7]=[CH:6][C:5]([N:8]=[S:9]([CH3:11])([N:13]([CH3:14])[CH3:12])=[O:10])=[CH:4][N:3]=1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 118863919HCID 118863919, compound

Product 1

HCID 118863962HCID 118863962, compound

Procedure

The title compound is prepared from N-(2-chloropyrimidin-5-yl)methanesulfinamide and dimethylamine following a procedure analogous to that described for Intermediate 3 (Step 2). LC (method 1): tR=0.72 min; Mass spectrum (ESI+): m/z=235 [M+H]+.

Sources & evidence

ORD record
ord-a37df47b6b0c4d769dedb66dc11a2ae4
Source dataset
uspto-grants-2016_08
Patent number
US09422312B2

Reaction notes

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