4-Bromobenzyl bromide → HCID 118863938, compound

HRID 1485644Notes

Reaction equation

HRID 1485644 reaction equation
[CH3:1][N:2]([CH3:7])[S:3]([CH3:6])(=[NH:5])=[O:4].[Br:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13]Br)=[CH:11][CH:10]=1.CN(C)S(C)(=NS(C1C=CC(C)=CC=1)(=O)=O)=O>>[Br:8][C:9]1[CH:16]=[CH:15][C:12]([CH2:13][N:5]=[S:3]([CH3:6])([N:2]([CH3:7])[CH3:1])=[O:4])=[CH:11][CH:10]=1

Participants

4

Reactant 3

HCID 685274-Bromobenzyl bromideHCID 12509541HCID 12509541, compoundHCID 118863948HCID 118863948, compound

Product 1

HCID 118863938HCID 118863938, compound

Procedure

The title compound is prepared from N,N-dimethyl-methanesulfonimidamide and 4-bromobenzyl bromide following a procedure analogous to that described for Intermediate 21 (Step 1). LC (method 1): tR=0.82 min; Mass spectrum (ESI+): m/z=291, 293 [M+H]+.

Sources & evidence

ORD record
ord-99769cc377f14ecba7892aaba2420b7b
Source dataset
uspto-grants-2016_08
Patent number
US09422312B2

Reaction notes

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