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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1485789Generated: October 31, 2026

Methyl chloroformate → HCID 118080634, compound

https://huagongshe.com/reaction/1485789

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl chloroformateHCID 6586—
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 118079199HCID 118079199—
ReactantHCID 118080534HCID 118080534—
ProductHCID 118080634HCID 118080634—

Reaction Steps

Isopropyl (S)-4-acetyl-6-((methoxycarbonyl)amino)-3-methyl-7-(4-(methylsulfonyl)phenyl)-3,4-dihydroquinoxaline-1(2H)-carboxylate was synthesized from isopropyl (S)-4-acetyl-6-amino-3-methyl-7-(4-(methylsulfonyl)phenyl)-3,4-dihydroquinoxaline-1(2H)-carboxylate and methyl chloroformate (instead of acetic anhydride) according to the procedure described above for isopropyl (S)-6-acetamido-4-acetyl-7-(1-cyclopropyl-1H-pyrazol-4-yl)-3-methyl-3,4-dihydroquinoxaline-1(2H)-carboxylate (Example 235). MS (ESI, pos. ion) m/z 504 [M+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09422281B2
Source datasetuspto-grants-2016_08
ORD IDord-12905f03cd98459ba69bc441a49856a6
Source noteuspto-grants-2016_08