N,N-Diethyl-beta-oxobenzenepropanamide → Dioxomolybdenum(VI) bis(N,N-diethyl-3-phenyl-3-oxopropane amidate)

HRID 1485916Notes

Reaction equation

HRID 1485916 reaction equation
O.O.[O-:3][Mo:4]([O-])(=O)=[O:5].[Na+].[Na+].[CH2:10]([N:12]([CH2:24][CH3:25])[C:13](=[O:23])[CH2:14][C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16])[CH3:11]>>[CH2:24]([N:12]([CH2:10][CH3:11])[C:13](=[O:23])[CH2:14][C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16])[CH3:25].[CH2:24]([N:12]([CH2:10][CH3:11])[C:13](=[O:23])[CH2:14][C:15]([C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)=[O:16])[CH3:25].[O:3]=[Mo+2:4]=[O:5]

Participants

3

Reactant 2

HCID 12196321N,N-Diethyl-beta-oxobenzenepropanamideHCID 16211258Sodium molybdate dihydrate

Product 1

HCID 131736770Dioxomolybdenum(VI) bis(N,N-diethyl-3-phenyl-3-oxopropane amidate)

Procedure

2.05 g sodium molybdate dihydrate and 4.33 g N,N-diethyl-3-phenyl-3-oxopropanamide were reacted according to General Preparation Procedure B. The product consisted of 5.18 g of a yellow, microcrystalline solid.

Workup

  1. customaccording to General Preparation Procedure B

Sources & evidence

ORD record
ord-8a131ff279c648a1b8841c496e35c91a
Source dataset
uspto-grants-2016_08
Patent number
US09422390B2

Reaction notes

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