HRID1486139

反应详情

EQUATION

反应方程式

HRID 1486139 反应方程式

PROCEDURE

实验过程

Prepared from 3-((2R)-2-(2-(trans-4-(tert-butoxycarbonylamino)cyclohexyl)acetamido)-2-(2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6.1.1.02,6]dec-4-yl)ethyl)-2-methoxybenzoic acid and BCl3 following the procedure described in Step 2 of Example 1. The crude product was purified by reverse phase preparative HPLC and dried using lyophilization. ESI-MS m/z 347 (MH)+.

WORKUP

后处理

  1. customThe crude product was purified by reverse phase preparative HPLC
  2. customdried