Trifluoroacetic acid → HCID 178520746, compound

Participants

Reaction Steps

To the compound from step 1 was added a mixture of TFA (2 mL) and H2O (0.2 mL). The resultant reaction mixture was stirred at RT for 2 hr. The solvents were then removed in vacuo and the residue purified by reverse phase preparative HPLC and dried using lyophilization. ESI-MS m/z 434 (MH)+.

Provenance & Evidence