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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1486366Generated: October 30, 2026

6-Bromohexanoic acid → HCID 178433620, compound

https://huagongshe.com/reaction/1486366

Reaction equation

Participants

RoleNameHCIDCharge
Reactant6-Bromohexanoic acidHCID 20210—
Reactant2,3,3-Trimethyl-3H-pyrrolo[2,3-b]pyridineHCID 22266836—
SolventEthyl AcetateHCID 8857—
ProductHCID 178433620HCID 178433620—

Reaction Conditions

Temperature120 °C

Reaction Steps

A mixture of 0.54 g of 2,3,3-trimethyl-3H-pyrrolo[2,3-b]pyridine and 1.32 g of 6-bromohexanoic acid is heated at 120° C. for one hair. Ethyl acetate (10 mL) is added, and the reaction mixture is heated at reflux for 15 minutes, then cooled to room temperature. The supernatant liquid is decanted to yield the product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09423323B2
Source datasetuspto-grants-2016_08
ORD IDord-0a9e4e28ef9b422a8acddc6b9aa21365
Source noteuspto-grants-2016_08