HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethanolamine → HCID 131736788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethanolamine | HCID 7618 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 131736788 | HCID 131736788 | — |
Reaction Steps
Into a 1 L flask, equipped with a refluxing condenser, is added 29.8 g (0.20 mole) of triethanolamine, 300 mL of dichloroethane, then 51.0 mL of thionyl chloride. The mixture is heated to reflux for 4 hrs. The reaction is quenched by adding 20 mL of methanol. Removal of solvent gives a white crystalline mass of tris(2-chloroethylamine) hydrochloride in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428450B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-f15408948ea24411944b92ea74fb83a8 |
| Source note | uspto-grants-2016_08 |