HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloropyrimidine → 5-(2-Chloro-pyrimidin-4-yl)-2-methoxy-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloropyrimidine | HCID 77531 | — |
| Reactant | (3-Formyl-4-methoxyphenyl)boronic acid | HCID 2759225 | — |
| Product | 5-(2-Chloro-pyrimidin-4-yl)-2-methoxy-benzaldehyde | HCID 53363596 | — |
Reaction Steps
2,4 dichloropyrimidine and 3-formyl 4-methoxy phenyl boronic acid were coupled following procedure A. LC-MS showed the product was >95% pure and had the expected M+H+ of 249.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07732444B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-8ef3cb688d8745649ceef176d6aa4eec |
| Source note | uspto-grants-2010_06 |