trans-2-Decenoic acid → 4-Benzyl-1-((E)-2-decenoyl)piperazine

HRID 1486621Notes

Reaction equation

HRID 1486621 reaction equation
[C:1]([OH:12])(=O)/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].Cl.Cl.[CH2:15]([N:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[CH2:15]([N:22]1[CH2:27][CH2:26][N:25]([C:1](=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])[CH2:24][CH2:23]1)[C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1

Participants

3

Reactant 2

HCID 5282724trans-2-Decenoic acidHCID 12198046Piperazine, 1-(phenylmethyl)-, hydrochloride (1:2)

Product 1

HCID 898815464-Benzyl-1-((E)-2-decenoyl)piperazine

Procedure

The same procedures as in Example 2 were carried out using (E)-2-decenoic acid and 1-benzylpiperazine dihydrochloride as starting raw materials, to produce an intended compound.

Workup

  1. customto produce an intended compound

Sources & evidence

ORD record
ord-7359f054d70d4db19f3b6dad9c00e58d
Source dataset
uspto-grants-2016_08
Patent number
US09428477B2

Reaction notes

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