trans-2-Decenoic acid → HCID 117920224, compound

HRID 1486628Notes

Reaction equation

HRID 1486628 reaction equation
[C:1]([OH:12])(=[O:11])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[ClH:13].Cl.[N:15]1([CH2:21][C:22]([O:24][CH2:25][CH3:26])=[O:23])[CH2:20][CH2:19][NH:18][CH2:17][CH2:16]1>>[C:1]([N:18]1[CH2:17][CH2:16][N:15]([CH2:21][C:22]([O:24][CH2:25][CH3:26])=[O:23])[CH2:20][CH2:19]1)(=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[ClH:13].[C:1]([N:18]1[CH2:17][CH2:16][N:15]([CH2:21][C:22]([OH:24])=[O:23])[CH2:20][CH2:19]1)(=[O:11])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 5282724trans-2-Decenoic acidHCID 117920701HCID 117920701, compound

Product 2

HCID 117920224HCID 117920224, compoundHCID 131736791HCID 131736791, compound

Procedure

The same procedures as in Example 2 were carried out using (E)-2-decenoic acid and ethyl 2-(1-piperazinyl)acetate dihydrochloride as starting raw materials, to produce ethyl [4-[(E)-2-decenoyl)piperazin-1-yl)acetate (ethyl ester of a free form of Compound 39).

Sources & evidence

ORD record
ord-888702f489f44f9ca27ed6af03f0667d
Source dataset
uspto-grants-2016_08
Patent number
US09428477B2

Reaction notes

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