trans-2-Decenoic acid → HCID 117920325, compound

HRID 1486629Notes

Reaction equation

HRID 1486629 reaction equation
[C:1]([OH:12])(=[O:11])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[ClH:13].Cl.[N:15]1([CH2:21][CH2:22][CH2:23][C:24]([O:26][CH2:27][CH3:28])=[O:25])[CH2:20][CH2:19][NH:18][CH2:17][CH2:16]1>>[C:1]([N:18]1[CH2:17][CH2:16][N:15]([CH2:21][CH2:22][CH2:23][C:24]([O:26][CH2:27][CH3:28])=[O:25])[CH2:20][CH2:19]1)(=[O:12])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[ClH:13].[C:1]([N:18]1[CH2:17][CH2:16][N:15]([CH2:21][CH2:22][CH2:23][C:24]([OH:26])=[O:25])[CH2:20][CH2:19]1)(=[O:11])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 5282724trans-2-Decenoic acidHCID 117920422HCID 117920422, compound

Product 2

HCID 117920325HCID 117920325, compoundHCID 117920494HCID 117920494, compound

Procedure

The same procedures as in Example 2 were carried out using (E)-2-decenoic acid and ethyl 4-(1-piperazinyl)butyrate dihydrochloride as starting raw materials, to produce ethyl 4-[4-((E)-2-decenoyl)piperazin-1-yl)butanoate (ethyl ester of a free form of Compound 40).

Sources & evidence

ORD record
ord-596fef22cf5141309851913392d1fe15
Source dataset
uspto-grants-2016_08
Patent number
US09428477B2

Reaction notes

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