HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Bromomethyl)-5-methyl-1,3-dioxol-2-one → HCID 72550983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Bromomethyl)-5-methyl-1,3-dioxol-2-one | HCID 10774141 | — |
| Reactant | HCID 117987534 | HCID 117987534 | — |
| Product | HCID 72550983 | HCID 72550983 | 29.3% |
Reaction Steps
(1S,2S,3S,5R,6S)-2-(((Allyloxy)carbonyl)amino)-3-fluorobicyclo[3.1.0]hexane-2,6-dicarboxylic acid (A-1-1, 660 mg) and 4-(bromomethyl)-5-methyl-1,3-dioxol-2-one (639 mg) were treated in the same manner as in Example A-1 (3) and (4) to give the title compound (C-2, 207 mg) as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428483B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-a24b495865cd4f898f17a400170dc5e6 |
| Source note | uspto-grants-2016_08 |