HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Chloro-3-nitrobenzaldehyde → HCID 86706528, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Chloro-3-nitrobenzaldehyde | HCID 85505 | — |
| Edukt | n-Cyclohexylpiperidine-4-carboxamide | HCID 12410238 | — |
| Edukt | HCID 86706529 | HCID 86706529 | — |
| Produkt | HCID 86706528 | HCID 86706528 | — |
Reaktionsschritte
The title compound is prepared according to the reactions described above starting from 4-chloro-3-nitro-benzaldehyde and piperidine-4-carboxylic acid cyclohexylamide yielding after reductive amination 1-(4-Chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide LC-MS A: tR=0.67 min; [M+H]+=380.03 and reduction with stannous chloride the title compound LC-MS A: tR=0.63 min; [M+H]+=350.21.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09428456B2 |
| Quelldatensatz | uspto-grants-2016_08 |
| ORD ID | ord-43632e1327164b87bd229c6014243e9d |
| Quellennotiz | uspto-grants-2016_08 |