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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1486698Erstellt: 25. Oktober 2026

4-Chloro-3-nitrobenzaldehyde → HCID 86706528, Verbindung

https://huagongshe.com/reaction/1486698

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt4-Chloro-3-nitrobenzaldehydeHCID 85505—
Eduktn-Cyclohexylpiperidine-4-carboxamideHCID 12410238—
EduktHCID 86706529HCID 86706529—
ProduktHCID 86706528HCID 86706528—

Reaktionsschritte

The title compound is prepared according to the reactions described above starting from 4-chloro-3-nitro-benzaldehyde and piperidine-4-carboxylic acid cyclohexylamide yielding after reductive amination 1-(4-Chloro-3-nitro-benzyl)-piperidine-4-carboxylic acid cyclohexylamide LC-MS A: tR=0.67 min; [M+H]+=380.03 and reduction with stannous chloride the title compound LC-MS A: tR=0.63 min; [M+H]+=350.21.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS09428456B2
Quelldatensatzuspto-grants-2016_08
ORD IDord-43632e1327164b87bd229c6014243e9d
Quellennotizuspto-grants-2016_08