Ethyl Acetate → HCID 89876011, compound

Participants

Reaction Steps

2-ethyl-N-isobutylaniline (83 mg, 0.468 mmol) was dissolved in pyridine (3 mL) add 4-vinylbenzene-1-sulfonyl chloride (114 mg, 0.562 mmol) added. Reaction stirred for over the weekend. Ethyl acetate (10 mL) was added to the solution and the organic phase was washed with water (10 mL), sodium hydroxide solution (2M, 2×10 mL) and brine (10 mL), then dried and concentrated under vacuum to provide the product, 129 mg. LCMS [LCMS1] Rt 1.43 min, m/z (ES+) 344 (M+H).

Provenance & Evidence