HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118061580, compound → HCID 118062084, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118061580 | HCID 118061580 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 118062084 | HCID 118062084 | 86.2% |
Reaction Steps
A solution of (1,1-dioxidothiazolidin-3-yl)(3-nitrophenyl)methanone (3 g, 11.10 mmol) in MeOH (30 ml) and 10% Pd—C (300 mg) was stirred under H2 (1 atm) for overnight. Reaction mixture was filtered through celite pad and the filtrate was evaporated under vacuum to afford the titled compound (2.3 gm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428499B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-305e1d4925f44d09af7c9407b8f5b91a |
| Source note | uspto-grants-2016_08 |