huagongshe.com
HRID1487885

反应详情

EQUATION

反应方程式

HRID 1487885 的结构方程式

REACTANTS

反应物

6
结构：CC(=N)N.Cl
HCID67170

Acetamidine hydrochloride

C2H7ClN2

结构：COC(=O)c1cccc(I)c1
HCID69258

Benzoic acid, 3-iodo-, methyl ester

C8H7IO2

结构：COCC(=N)N.Cl
HCID13548602

Methoxyethanimidamide--hydrogen chloride (1/1)

C3H9ClN2O

结构：COC(=O)c1ccc(C)c(I)c1
HCID13614033

Methyl 3-iodo-4-methylbenzoate

C9H9IO2

结构：Cl.N#Cc1ccc(C2CCNCC2)cc1
HCID19391618

4-(Piperidin-4-yl)benzonitrile--hydrogen chloride (1/1)

C12H15ClN2

结构：Cl.N#Cc1ccc(C2CNC2)cc1
HCID55254991

未命名化合物

2 次

PRODUCTS

生成物

1
结构：Cc1nc(Cl)c(-c2cccc(C(=O)N3CC(c4ccc(C#N)cc4)C3)c2)[nH]1
HCID178432857

未命名化合物

PROCEDURE

实验过程

The title compound was prepared using standard chemical manipulations and procedures similar to those used for preparation of compound 27, except methyl 3-iodobenzoate was used in place of methyl 3-iodo-4-methylbenzoate (compound 5.3), acetimidamide hydrochloride was used in place of 2-methoxyacetimidamide (compound 4.7) and 4-(azetidin-3-yl)benzonitrile hydrochloride (compound 5.2) was used in place of 4-(piperidin-4-yl)benzonitrile hydrochloride (compound 1.2). m/z (ES+) 377 (M+H)+.