HCID 178432771, compound → HCID 178497724, compound

HRID 1487916Notes

Reaction equation

HRID 1487916 reaction equation
CC1[NH:3][C:4]([C:8]2[CH:9]=[C:10]([CH:15]=[CH:16][C:17]=2[CH3:18])[C:11]([O:13][CH3:14])=[O:12])=[C:5]([CH3:7])N=1.IC1N[N:23]=[C:22](C)[C:21]=1C.IC1NC(C)=NC=1C>>[CH3:21][C:22]1[C:5]([CH3:7])=[C:4]([C:8]2[CH:9]=[C:10]([CH:15]=[CH:16][C:17]=2[CH3:18])[C:11]([O:13][CH3:14])=[O:12])[NH:3][N:23]=1

Participants

4

Reactant 3

HCID 178432771HCID 178432771, compoundHCID 178434628HCID 178434628, compound2×HCID 178497719HCID 178497719, compound

Product 1

HCID 178497724HCID 178497724, compound

Procedure

The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 5.6, except 5-iodo-3,4-dimethyl-1H-pyrazole (compound 59.1) was used in place of 5-iodo-2,4-dimethyl-1H-imidazole (compound 5.5). m/z (ES+) 245 (M+H)+.

Sources & evidence

ORD record
ord-ac9d8b4e48104147992417ce12d2c91f
Source dataset
uspto-grants-2016_08
Patent number
US09428502B2

Reaction notes

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