HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 3-iodo-4-methylbenzoate → Methyl 2,4-dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 3-iodo-4-methylbenzoate | HCID 13614033 | — |
| Reactant | Methyl 5-iodo-2,4-dimethylbenzoate | HCID 44828936 | — |
| Reactant | 5-Methoxycarbonyl-2-methylphenylboronic acid pinacol ester | HCID 53217136 | — |
| Product | Methyl 2,4-dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate | HCID 59224686 | — |
Reaction Steps
The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 5.4, except methyl 5-iodo-2,4-dimethylbenzoate (compound 31.1) was used in place of methyl 3-iodo-4-methylbenzoate (compound 5.3). m/z (ES+) 291(M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428502B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-154dfedacaa44dabbd498aae92a58b44 |
| Source note | uspto-grants-2016_08 |