HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methoxycarbonyl-2-methylphenylboronic acid pinacol ester → HCID 178497346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methoxycarbonyl-2-methylphenylboronic acid pinacol ester | HCID 53217136 | — |
| Reactant | Methyl 2,4-dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate | HCID 59224686 | — |
| Reactant | HCID 178432598 | HCID 178432598 | — |
| Reactant | HCID 178432771 | HCID 178432771 | — |
| Reactant | HCID 178497719 | HCID 178497719 | — |
| Product | HCID 178497346 | HCID 178497346 | — |
Reaction Steps
The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 5.6, except methyl 2,4-dimethyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate (compound 160.1) was used in place of methyl 4-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate (compound 5.4) and 5-iodo-4-methyl-2-(3-methyloxetan-3-yl)-1H-imidazole (compound 175.2) was used in place of 5-iodo-2,4-dimethyl-1H-imidazole (compound 5.5). m/z (ES+) 315 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09428502B2 |
| Source dataset | uspto-grants-2016_08 |
| ORD ID | ord-112d9e9e2d734563a3271cfba99cc6d6 |
| Source note | uspto-grants-2016_08 |