HCID 178430849, compound → HCID 178432633, compound

HRID 1488041Notes

Reaction equation

HRID 1488041 reaction equation
[I:1][C:2]1[NH:6][C:5]([C:7]2(C)[CH2:10][O:9][CH2:8]2)=[N:4][C:3]=1[CH3:12].CC1N=C(C2COC2)NC=1.CC1N=C(C2(C)COC2)NC=1>>[I:1][C:2]1[NH:6][C:5]([CH:7]2[CH2:10][O:9][CH2:8]2)=[N:4][C:3]=1[CH3:12]

Participants

4

Reactant 3

HCID 178430849HCID 178430849, compoundHCID 178430860HCID 178430860, compound2×HCID 178432598HCID 178432598, compound

Product 1

HCID 178432633HCID 178432633, compound

Procedure

The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 175.2, except 4-methyl-2-(oxetan-3-yl)-1H-imidazole (compound 180.1) was used in place of 4-methyl-2-(3-methyloxetan-3-yl)-1H-imidazole (compound 175.1). m/z (ES+) 265 (M+H)+.

Sources & evidence

ORD record
ord-f3e7dc7fe2cc4d18be8762643ce5066e
Source dataset
uspto-grants-2016_08
Patent number
US09428502B2

Reaction notes

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