HCID 178425892, compound → HCID 178424694, compound

HRID 1488136Notes

Reaction equation

HRID 1488136 reaction equation
CC1C(C)=C(C2C=C(C=CC=2C)C(O)=O)NN=1.[CH3:18][C:19]1[C:23]([CH3:24])=[C:22]([C:25]2[C:26]([CH3:36])=[CH:27][C:28]([CH3:35])=[C:29]([CH:34]=2)[C:30]([O:32]C)=[O:31])[NH:21][N:20]=1.CC1C(C)=C(C2C=C(C=CC=2C)C(OC)=O)NN=1>>[CH3:18][C:19]1[C:23]([CH3:24])=[C:22]([C:25]2[C:26]([CH3:36])=[CH:27][C:28]([CH3:35])=[C:29]([CH:34]=2)[C:30]([OH:32])=[O:31])[NH:21][N:20]=1

Participants

4

Reactant 3

HCID 178425892HCID 178425892, compoundHCID 178497390HCID 178497390, compound2×HCID 178497724HCID 178497724, compound

Product 1

HCID 178424694HCID 178424694, compound

Procedure

The title compound was prepared using standard chemical manipulations and procedures similar to those used for the preparation of compound 59.3, except methyl 5-(3,4-dimethyl-1H-pyrazol-5-yl)-2,4-dimethylbenzoate (compound 242.1) was used in place of methyl 3-(3,4-dimethyl-1H-pyrazol-5-yl)-4-methylbenzoate (compound 59.2). m/z (ES+) 245 (M+H)+.

Sources & evidence

ORD record
ord-0a14cf7ab27d4490896793cb57ff4fdd
Source dataset
uspto-grants-2016_08
Patent number
US09428502B2

Reaction notes

Loading…