HCID 122605067, compound → HCID 117996327, compound

Participants

Reaction Steps

In a 100 mL flask, N2-[(benzyloxy)carbonyl]-N6-[6-({2-[(α-L-fucopyranosyl)oxy]ethyl}amino)-6-oxohexanoyl]-L-lysine (200 mg, 0.335 mmol) was dissolved in water (5 mL). The flask was degassed and filled with N2. To the above mixture was added PdOH2 (48.7 mg, 0.069 mmol. The mixture was stirred under H2 balloon for 2 hr. The mixture was filtered through a pad of Celite, and the filtrate was concentrated to give the title compound. UPLC Method B: m/e=464.2697 [M+1]; Rt=2.61 min.

Provenance & Evidence