Benzene → Tridecane

HRID 1488367Notes

Reaction equation

HRID 1488367 reaction equation
N1[CH2:12][CH2:11]NCCNCCNCC1.[CH:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>>[CH3:15][CH2:14][CH2:13][CH2:18][CH2:17][CH2:13][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:11][CH3:12]

Participants

3

Reactant 2

HCID 241BenzeneHCID 649631,4,7,10-Tetraazacyclododecane

Product 1

HCID 12388Tridecane

Procedure

reacting 1,4,7,10 tetraazacyclododecane with dimethylformamidedimethylacetal in the presence of benzene to yield 1,4,7,10 tetraazatricyclo(5.5.1.0)tridecane,

Sources & evidence

ORD record
ord-9ccce9edbc6143be8772245db57f0be4
Source dataset
uspto-grants-1997_10
Patent number
US05674470

Reaction notes

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