Sodium Hydroxide → HCID 70059029, compound

HRID 1488713Notes

Reaction equation

HRID 1488713 reaction equation
[OH-].[Na+].[CH2:3]([N:6]([C@H:28]1[CH2:37][CH2:36][C:35]2[C:30](=[CH:31][CH:32]=[C:33]([O:46][CH2:47][C:48]3[CH:53]=[CH:52][CH:51]=[CH:50][CH:49]=3)[C:34]=2[O:38][CH2:39][C:40]2[CH:45]=[CH:44][CH:43]=[CH:42][CH:41]=2)[CH2:29]1)[C:7](=[O:27])[CH2:8][CH2:9][CH2:10][CH2:11][C:12]([NH:14][CH2:15][CH2:16][C:17]1[CH:22]=[CH:21][C:20]([C:23]([O:25]C)=[O:24])=[CH:19][CH:18]=1)=[O:13])[CH2:4][CH3:5]>CO>[CH2:3]([N:6]([C@H:28]1[CH2:37][CH2:36][C:35]2[C:30](=[CH:31][CH:32]=[C:33]([O:46][CH2:47][C:48]3[CH:49]=[CH:50][CH:51]=[CH:52][CH:53]=3)[C:34]=2[O:38][CH2:39][C:40]2[CH:41]=[CH:42][CH:43]=[CH:44][CH:45]=2)[CH2:29]1)[C:7](=[O:27])[CH2:8][CH2:9][CH2:10][CH2:11][C:12]([NH:14][CH2:15][CH2:16][C:17]1[CH:18]=[CH:19][C:20]([C:23]([OH:25])=[O:24])=[CH:21][CH:22]=1)=[O:13])[CH2:4][CH3:5]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 70192059HCID 70192059, compound

Product 1

HCID 70059029HCID 70059029, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

An aqueous solution of NaOH 4N (2 ml) was added dropwise at room temperature to a stirred solution of Intermediate 56 (2.0 g; 2.9 mmoles), prepared as described in example 26, in methanol (10 ml).

Workup

  1. customprepared

Sources & evidence

ORD record
ord-47aa28efbc0045148b646f93b9dc86b6
Source dataset
uspto-grants-1997_10
Patent number
US05674909

Reaction notes

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